Preparação e caracterização espectroscópica de complexos de boro: uma proposta para uma prática integrada de química inorgânica
Đã lưu trong:
| Tác giả chính: | |
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| Ngày xuất bản: | 2010 |
| Tác giả khác: | , , , |
| Định dạng: | Article |
| Ngôn ngữ: | por |
| Nguồn: | Repositório Institucional da UnB |
| Download full: | http://repositorio.unb.br/handle/10482/27651 https://dx.doi.org/10.1590/S0100-40422010000600034 |
Tóm tắt: | As a proposal for an undergraduate second or third year inorganic laboratory course, the present paper describes the preparation of three representative boron complexes: potassium tetrafluoroborate, pyridoxin boron complex and potassium bis(oxalato)borate. The complexes are characterised by infrared and multinuclear magnetic resonance spectroscopy (¹H, 11B and 19F) where isotopic effects are demonstrated. |
| Tóm tắt: | As a proposal for an undergraduate second or third year inorganic laboratory course, the present paper describes the preparation of three representative boron complexes: potassium tetrafluoroborate, pyridoxin boron complex and potassium bis(oxalato)borate. The complexes are characterised by infrared and multinuclear magnetic resonance spectroscopy (¹H, 11B and 19F) where isotopic effects are demonstrated. |
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