Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion

Bibliographic Details
Main Author: Kugelmeier, C. L.
Publication Date: 2024
Other Authors: Unti, L. F.K., Júnior, E. L.S., Souza, N. M., Jardini, A. L., Avila, J. A. [UNESP], Cintho, O. M., Zilnyk, K.
Format: Article
Language: eng
Source: Repositório Institucional da UNESP
Download full: http://dx.doi.org/10.1007/s11665-024-09769-w
https://hdl.handle.net/11449/305774
Summary: Precipitation hardening (PH) martensitic stainless steels, such as 17-4, have been investigated for use in additive manufacturing (AM) techniques to produce parts with complex and individualized geometries, finding wide use in the aerospace, petrochemical, nuclear, and marine industries due to their high mechanical strength and corrosion resistance. However, AM can result in a material with the presence of porosities, segregations and metastable phases. Thus, the aim of this research is to study the microstructure evolution and corrosion resistance of 17-4 PH processed by laser powder bed fusion (LPBF) in comparison with conventional processing, under thermal treatment, as-built, and after AM processing with thermal treatment conditions. The findings of this study show that the AM-processed material exhibits a microstructure with a fish scale-like morphology, smaller grain size and higher fraction of retained austenite, characteristics that are modified after solubilization treatment, although the hardness remains higher than that observed in conventional processing. The corrosion test results showed that the samples treated after AM processing present a corrosion resistance close to the samples only thermally treated.
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spelling Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion17-4 PH stainless steeladditive manufacturingcorrosion resistanceengineering materiallaser powder bed fusionPrecipitation hardening (PH) martensitic stainless steels, such as 17-4, have been investigated for use in additive manufacturing (AM) techniques to produce parts with complex and individualized geometries, finding wide use in the aerospace, petrochemical, nuclear, and marine industries due to their high mechanical strength and corrosion resistance. However, AM can result in a material with the presence of porosities, segregations and metastable phases. Thus, the aim of this research is to study the microstructure evolution and corrosion resistance of 17-4 PH processed by laser powder bed fusion (LPBF) in comparison with conventional processing, under thermal treatment, as-built, and after AM processing with thermal treatment conditions. The findings of this study show that the AM-processed material exhibits a microstructure with a fish scale-like morphology, smaller grain size and higher fraction of retained austenite, characteristics that are modified after solubilization treatment, although the hardness remains higher than that observed in conventional processing. The corrosion test results showed that the samples treated after AM processing present a corrosion resistance close to the samples only thermally treated.Department of Mechanical Engineering Aeronautics Institute of Technology (ITA), SPAeronautics Institute of Technology (ITA) Postgraduate Program in Aeronautical and Mechanical Engineering (PG/EAM), SPBIOFABRIS - National Institute of Science and Technology in Biomanufacturing Faculty of Chemical Engineering University of Campinas, SPSchool of Engineering Universidade Estadual Paulista (Unesp), SPDepartment of Materials Engineering State University of Ponta Grossa (UEPG), PRSchool of Engineering Universidade Estadual Paulista (Unesp), SPAeronautics Institute of Technology (ITA)Postgraduate Program in Aeronautical and Mechanical Engineering (PG/EAM)Universidade Estadual de Campinas (UNICAMP)Universidade Estadual Paulista (UNESP)Universidade Estadual de Ponta Grossa (UEPG)Kugelmeier, C. L.Unti, L. F.K.Júnior, E. L.S.Souza, N. M.Jardini, A. L.Avila, J. A. [UNESP]Cintho, O. M.Zilnyk, K.2025-04-29T20:04:10Z2024-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articlehttp://dx.doi.org/10.1007/s11665-024-09769-wJournal of Materials Engineering and Performance.1544-10241059-9495https://hdl.handle.net/11449/30577410.1007/s11665-024-09769-w2-s2.0-85197408497Scopusreponame:Repositório Institucional da UNESPinstname:Universidade Estadual Paulista (UNESP)instacron:UNESPengJournal of Materials Engineering and Performanceinfo:eu-repo/semantics/openAccess2025-04-30T14:32:30Zoai:repositorio.unesp.br:11449/305774Repositório InstitucionalPUBhttp://repositorio.unesp.br/oai/requestrepositoriounesp@unesp.bropendoar:29462025-04-30T14:32:30Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)false
dc.title.none.fl_str_mv Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion
title Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion
spellingShingle Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion
Kugelmeier, C. L.
17-4 PH stainless steel
additive manufacturing
corrosion resistance
engineering material
laser powder bed fusion
title_short Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion
title_full Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion
title_fullStr Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion
title_full_unstemmed Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion
title_sort Microstructure Evolution and Corrosion Resistance Evaluation of 17-4 Precipitation Hardening Stainless Steel Processed by Laser Powder Bed Fusion
author Kugelmeier, C. L.
author_facet Kugelmeier, C. L.
Unti, L. F.K.
Júnior, E. L.S.
Souza, N. M.
Jardini, A. L.
Avila, J. A. [UNESP]
Cintho, O. M.
Zilnyk, K.
author_role author
author2 Unti, L. F.K.
Júnior, E. L.S.
Souza, N. M.
Jardini, A. L.
Avila, J. A. [UNESP]
Cintho, O. M.
Zilnyk, K.
author2_role author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Aeronautics Institute of Technology (ITA)
Postgraduate Program in Aeronautical and Mechanical Engineering (PG/EAM)
Universidade Estadual de Campinas (UNICAMP)
Universidade Estadual Paulista (UNESP)
Universidade Estadual de Ponta Grossa (UEPG)
dc.contributor.author.fl_str_mv Kugelmeier, C. L.
Unti, L. F.K.
Júnior, E. L.S.
Souza, N. M.
Jardini, A. L.
Avila, J. A. [UNESP]
Cintho, O. M.
Zilnyk, K.
dc.subject.por.fl_str_mv 17-4 PH stainless steel
additive manufacturing
corrosion resistance
engineering material
laser powder bed fusion
topic 17-4 PH stainless steel
additive manufacturing
corrosion resistance
engineering material
laser powder bed fusion
description Precipitation hardening (PH) martensitic stainless steels, such as 17-4, have been investigated for use in additive manufacturing (AM) techniques to produce parts with complex and individualized geometries, finding wide use in the aerospace, petrochemical, nuclear, and marine industries due to their high mechanical strength and corrosion resistance. However, AM can result in a material with the presence of porosities, segregations and metastable phases. Thus, the aim of this research is to study the microstructure evolution and corrosion resistance of 17-4 PH processed by laser powder bed fusion (LPBF) in comparison with conventional processing, under thermal treatment, as-built, and after AM processing with thermal treatment conditions. The findings of this study show that the AM-processed material exhibits a microstructure with a fish scale-like morphology, smaller grain size and higher fraction of retained austenite, characteristics that are modified after solubilization treatment, although the hardness remains higher than that observed in conventional processing. The corrosion test results showed that the samples treated after AM processing present a corrosion resistance close to the samples only thermally treated.
publishDate 2024
dc.date.none.fl_str_mv 2024-01-01
2025-04-29T20:04:10Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://dx.doi.org/10.1007/s11665-024-09769-w
Journal of Materials Engineering and Performance.
1544-1024
1059-9495
https://hdl.handle.net/11449/305774
10.1007/s11665-024-09769-w
2-s2.0-85197408497
url http://dx.doi.org/10.1007/s11665-024-09769-w
https://hdl.handle.net/11449/305774
identifier_str_mv Journal of Materials Engineering and Performance.
1544-1024
1059-9495
10.1007/s11665-024-09769-w
2-s2.0-85197408497
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Journal of Materials Engineering and Performance
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.source.none.fl_str_mv Scopus
reponame:Repositório Institucional da UNESP
instname:Universidade Estadual Paulista (UNESP)
instacron:UNESP
instname_str Universidade Estadual Paulista (UNESP)
instacron_str UNESP
institution UNESP
reponame_str Repositório Institucional da UNESP
collection Repositório Institucional da UNESP
repository.name.fl_str_mv Repositório Institucional da UNESP - Universidade Estadual Paulista (UNESP)
repository.mail.fl_str_mv repositoriounesp@unesp.br
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