A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid

Bibliographic Details
Main Author: Umer,Asim
Publication Date: 2014
Other Authors: Naveed,Shahid, Ramzan,Naveed, Rafique,Muhammad Shahid, Imran,Muhammad
Format: Article
Language: eng
Source: Matéria (Rio de Janeiro. Online)
Download full: http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762014000300197
Summary: Chemical Reduction technique was employed to prepared highly stable and dispersed Copper nanoparticles using L-Ascorbic Acid (Vitamin C) as reducing as well as capping agent. In this technique, cupric chloride was used as precursor. The effects of different molar ratios of L-Ascorbic Acid on the concentration and size of copper nanoparticles were studied. The Copper nanoparticles were characterized by X-Ray Diffraction, Atomic Absorption Spectrometry, and Fourier Transform Infrared Spectrometry. The results show that with the increase in the molar ratio of L-ascorbic acid the concentration of Copper nanoparticles were also increased. The average particles size of copper nanoparticle was found in the range of 50-60 nm. The product was kept in ambient conditions for three month but no sedimentation or separation was observed. The use of ascorbic acid makes the process a non-toxic, cost effective and environmental friendly green method.
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spelling A green method for the synthesis of Copper Nanoparticles using L-ascorbic acidCopper nanoparticlesascorbic acidcopper saltXRDFTIRChemical Reduction technique was employed to prepared highly stable and dispersed Copper nanoparticles using L-Ascorbic Acid (Vitamin C) as reducing as well as capping agent. In this technique, cupric chloride was used as precursor. The effects of different molar ratios of L-Ascorbic Acid on the concentration and size of copper nanoparticles were studied. The Copper nanoparticles were characterized by X-Ray Diffraction, Atomic Absorption Spectrometry, and Fourier Transform Infrared Spectrometry. The results show that with the increase in the molar ratio of L-ascorbic acid the concentration of Copper nanoparticles were also increased. The average particles size of copper nanoparticle was found in the range of 50-60 nm. The product was kept in ambient conditions for three month but no sedimentation or separation was observed. The use of ascorbic acid makes the process a non-toxic, cost effective and environmental friendly green method.Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiroem cooperação com a Associação Brasileira do Hidrogênio, ABH22014-09-01info:eu-repo/semantics/articleinfo:eu-repo/semantics/publishedVersiontext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762014000300197Matéria (Rio de Janeiro) v.19 n.3 2014reponame:Matéria (Rio de Janeiro. Online)instname:Matéria (Rio de Janeiro. Online)instacron:RLAM10.1590/S1517-70762014000300002info:eu-repo/semantics/openAccessUmer,AsimNaveed,ShahidRamzan,NaveedRafique,Muhammad ShahidImran,Muhammadeng2015-10-09T00:00:00Zoai:scielo:S1517-70762014000300197Revistahttp://www.materia.coppe.ufrj.br/https://old.scielo.br/oai/scielo-oai.php||materia@labh2.coppe.ufrj.br1517-70761517-7076opendoar:2015-10-09T00:00Matéria (Rio de Janeiro. Online) - Matéria (Rio de Janeiro. Online)false
dc.title.none.fl_str_mv A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid
title A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid
spellingShingle A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid
Umer,Asim
Copper nanoparticles
ascorbic acid
copper salt
XRD
FTIR
title_short A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid
title_full A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid
title_fullStr A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid
title_full_unstemmed A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid
title_sort A green method for the synthesis of Copper Nanoparticles using L-ascorbic acid
author Umer,Asim
author_facet Umer,Asim
Naveed,Shahid
Ramzan,Naveed
Rafique,Muhammad Shahid
Imran,Muhammad
author_role author
author2 Naveed,Shahid
Ramzan,Naveed
Rafique,Muhammad Shahid
Imran,Muhammad
author2_role author
author
author
author
dc.contributor.author.fl_str_mv Umer,Asim
Naveed,Shahid
Ramzan,Naveed
Rafique,Muhammad Shahid
Imran,Muhammad
dc.subject.por.fl_str_mv Copper nanoparticles
ascorbic acid
copper salt
XRD
FTIR
topic Copper nanoparticles
ascorbic acid
copper salt
XRD
FTIR
description Chemical Reduction technique was employed to prepared highly stable and dispersed Copper nanoparticles using L-Ascorbic Acid (Vitamin C) as reducing as well as capping agent. In this technique, cupric chloride was used as precursor. The effects of different molar ratios of L-Ascorbic Acid on the concentration and size of copper nanoparticles were studied. The Copper nanoparticles were characterized by X-Ray Diffraction, Atomic Absorption Spectrometry, and Fourier Transform Infrared Spectrometry. The results show that with the increase in the molar ratio of L-ascorbic acid the concentration of Copper nanoparticles were also increased. The average particles size of copper nanoparticle was found in the range of 50-60 nm. The product was kept in ambient conditions for three month but no sedimentation or separation was observed. The use of ascorbic acid makes the process a non-toxic, cost effective and environmental friendly green method.
publishDate 2014
dc.date.none.fl_str_mv 2014-09-01
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762014000300197
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762014000300197
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 10.1590/S1517-70762014000300002
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro
em cooperação com a Associação Brasileira do Hidrogênio, ABH2
publisher.none.fl_str_mv Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro
em cooperação com a Associação Brasileira do Hidrogênio, ABH2
dc.source.none.fl_str_mv Matéria (Rio de Janeiro) v.19 n.3 2014
reponame:Matéria (Rio de Janeiro. Online)
instname:Matéria (Rio de Janeiro. Online)
instacron:RLAM
instname_str Matéria (Rio de Janeiro. Online)
instacron_str RLAM
institution RLAM
reponame_str Matéria (Rio de Janeiro. Online)
collection Matéria (Rio de Janeiro. Online)
repository.name.fl_str_mv Matéria (Rio de Janeiro. Online) - Matéria (Rio de Janeiro. Online)
repository.mail.fl_str_mv ||materia@labh2.coppe.ufrj.br
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