3-(Ammoniomethyl)pyridinium bis(perchlorate)

Bibliographic Details
Main Author: Bayar, Imen
Publication Date: 2013
Other Authors: Kefi, Riadh, Silva, Pedro Sidónio Pereira da, Silva, Manuela Ramos
Format: Article
Language: eng
Source: Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
Download full: https://hdl.handle.net/10316/27498
https://doi.org/10.1107/S1600536813012038
Summary: In the title molecular salt, C6H10N2 2+ 2ClO4 , the Cl—O bond lengths [anion 1: 1.369 (3)–1.415 (3); anion 2: 1.420 (2)– 1.441 (2) A ° ] and the O—Cl—O angles [anion 1: 105.4 (2)– 111.8 (4); anion 2: 107.8 (1)–110.3 (1) ] indicate a slight distortion of the perchlorate anions from regular tetrahedral symmetry. In the crystal, the components are linked into columns along the a-axis direction via N—H O and C— H O hydrogen bonds, with stacks of the organic molecules being surrounded by stacks of perchlorate anions.
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spelling 3-(Ammoniomethyl)pyridinium bis(perchlorate)single-crystal X-ray studyT = 293 Kmean (C–C) = 0.003 AR factor = 0.051wR factor = 0.148data-to-parameter ratio = 21.5In the title molecular salt, C6H10N2 2+ 2ClO4 , the Cl—O bond lengths [anion 1: 1.369 (3)–1.415 (3); anion 2: 1.420 (2)– 1.441 (2) A ° ] and the O—Cl—O angles [anion 1: 105.4 (2)– 111.8 (4); anion 2: 107.8 (1)–110.3 (1) ] indicate a slight distortion of the perchlorate anions from regular tetrahedral symmetry. In the crystal, the components are linked into columns along the a-axis direction via N—H O and C— H O hydrogen bonds, with stacks of the organic molecules being surrounded by stacks of perchlorate anions.2013info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articlehttps://hdl.handle.net/10316/27498https://hdl.handle.net/10316/27498https://doi.org/10.1107/S1600536813012038engBAYAR, Imen [et. al] - 3-(Ammoniomethyl)pyridinium bis(perchlorate). "Acta Crystallographica Section E". ISSN 1600-5368. Vol. 69 (2013)1600-5368http://scripts.iucr.org/cgi-bin/paper?S1600536813012038Bayar, ImenKefi, RiadhSilva, Pedro Sidónio Pereira daSilva, Manuela Ramosinfo:eu-repo/semantics/openAccessreponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiainstacron:RCAAP2021-10-28T09:11:55Zoai:estudogeral.uc.pt:10316/27498Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireinfo@rcaap.ptopendoar:https://opendoar.ac.uk/repository/71602025-05-29T05:21:59.705081Repositórios Científicos de Acesso Aberto de Portugal (RCAAP) - FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiafalse
dc.title.none.fl_str_mv 3-(Ammoniomethyl)pyridinium bis(perchlorate)
title 3-(Ammoniomethyl)pyridinium bis(perchlorate)
spellingShingle 3-(Ammoniomethyl)pyridinium bis(perchlorate)
Bayar, Imen
single-crystal X-ray study
T = 293 K
mean (C–C) = 0.003 A
R factor = 0.051
wR factor = 0.148
data-to-parameter ratio = 21.5
title_short 3-(Ammoniomethyl)pyridinium bis(perchlorate)
title_full 3-(Ammoniomethyl)pyridinium bis(perchlorate)
title_fullStr 3-(Ammoniomethyl)pyridinium bis(perchlorate)
title_full_unstemmed 3-(Ammoniomethyl)pyridinium bis(perchlorate)
title_sort 3-(Ammoniomethyl)pyridinium bis(perchlorate)
author Bayar, Imen
author_facet Bayar, Imen
Kefi, Riadh
Silva, Pedro Sidónio Pereira da
Silva, Manuela Ramos
author_role author
author2 Kefi, Riadh
Silva, Pedro Sidónio Pereira da
Silva, Manuela Ramos
author2_role author
author
author
dc.contributor.author.fl_str_mv Bayar, Imen
Kefi, Riadh
Silva, Pedro Sidónio Pereira da
Silva, Manuela Ramos
dc.subject.por.fl_str_mv single-crystal X-ray study
T = 293 K
mean (C–C) = 0.003 A
R factor = 0.051
wR factor = 0.148
data-to-parameter ratio = 21.5
topic single-crystal X-ray study
T = 293 K
mean (C–C) = 0.003 A
R factor = 0.051
wR factor = 0.148
data-to-parameter ratio = 21.5
description In the title molecular salt, C6H10N2 2+ 2ClO4 , the Cl—O bond lengths [anion 1: 1.369 (3)–1.415 (3); anion 2: 1.420 (2)– 1.441 (2) A ° ] and the O—Cl—O angles [anion 1: 105.4 (2)– 111.8 (4); anion 2: 107.8 (1)–110.3 (1) ] indicate a slight distortion of the perchlorate anions from regular tetrahedral symmetry. In the crystal, the components are linked into columns along the a-axis direction via N—H O and C— H O hydrogen bonds, with stacks of the organic molecules being surrounded by stacks of perchlorate anions.
publishDate 2013
dc.date.none.fl_str_mv 2013
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv https://hdl.handle.net/10316/27498
https://hdl.handle.net/10316/27498
https://doi.org/10.1107/S1600536813012038
url https://hdl.handle.net/10316/27498
https://doi.org/10.1107/S1600536813012038
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv BAYAR, Imen [et. al] - 3-(Ammoniomethyl)pyridinium bis(perchlorate). "Acta Crystallographica Section E". ISSN 1600-5368. Vol. 69 (2013)
1600-5368
http://scripts.iucr.org/cgi-bin/paper?S1600536813012038
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.source.none.fl_str_mv reponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron:RCAAP
instname_str FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron_str RCAAP
institution RCAAP
reponame_str Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
collection Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
repository.name.fl_str_mv Repositórios Científicos de Acesso Aberto de Portugal (RCAAP) - FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
repository.mail.fl_str_mv info@rcaap.pt
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