Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system

Bibliographic Details
Main Author: Halla, Noureddine
Publication Date: 2017
Other Authors: Fernandes, Isabel P., Heleno, Sandrina A., Calhelha, Ricardo C., Costa, Patrícia, Rodrigues, Alírio, Boucherit, Kebir, Ferreira, Isabel C.F.R., Barreiro, M.F.
Language: eng
Source: Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
Download full: http://hdl.handle.net/10198/14525
Summary: A. leucotrichus (Coss. & Dur.) Coss. & Dur., known in Algeria as “Kammûnes-sofi”, is a medicinal plant that finds culinary use by indigenous populations. Among others, it is used against stomach pain, indigestion, diarrhea, vomiting, fever, and to combat high blood pressure. In this work, the essential oil of A. leucotrichus, obtained by steam distillation (3h) from fruits collected in March 2015 from Tassili n'Ajjer, a vast plateau in south-east Algeria (25°30'0" N and 9°0'0" E), was chemically and biologically characterized and thereafter microencapsulated using a chitosan/TPP/vanillin system.
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spelling Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical systemMicroencapsulationChitosan/TPP/vanillinA. leucotrichus (Coss. & Dur.) Coss. & Dur., known in Algeria as “Kammûnes-sofi”, is a medicinal plant that finds culinary use by indigenous populations. Among others, it is used against stomach pain, indigestion, diarrhea, vomiting, fever, and to combat high blood pressure. In this work, the essential oil of A. leucotrichus, obtained by steam distillation (3h) from fruits collected in March 2015 from Tassili n'Ajjer, a vast plateau in south-east Algeria (25°30'0" N and 9°0'0" E), was chemically and biologically characterized and thereafter microencapsulated using a chitosan/TPP/vanillin system.A. leucotrichus essential oil microparticles were produced using an atomization/coagulation technique with chitosan as the shell material, sodium tripolyphosphaste (TPP) and vanillin as crosslinking agents. Comparatively to the most used chemical systems, this one presents several advantages since all the raw materials are nontoxic and no organic solvents are required. Moreover, the used microencapsulation process allows the microparticles production in a single step, without having the constrains of the traditionally used oil-in-water (o/w) emulsion based techniques. The adopted procedure comprises the following stages: (1) Chitosan solution (CS) preparation (3.0%, w/v) in acidic medium (acetic acid 3%, v/v); (2) Oil-in-water (o/w) emulsion preparation by emulsifying the essential oil (O) with the chitosan solution at O/CS ratio of 0.025 (v/v) with Tween 80 (emulsifier of HLB=15.0, 1.5%, w/v). The emulsion was homogenized at 11000 rpm during 5 min with a CAT Unidrive X homogenizer; (3) Atomization of the o/w emulsion in a Nisco VarJ30 system (flow rate: 0.3 ml/min) under pressurized nitrogen; (4) Coagulation with TPP (10%, w/v at pH 6.0) followed by vanillin crosslinking (1.0% (w/v), 50ºC at 0.5 ml/min during 2 h). Microparticles were recovered by filtration under reduced pressure, washed with distilled water and stored in the hydrated form.SPQBiblioteca Digital do IPBHalla, NoureddineFernandes, Isabel P.Heleno, Sandrina A.Calhelha, Ricardo C.Costa, PatríciaRodrigues, AlírioBoucherit, KebirFerreira, Isabel C.F.R.Barreiro, M.F.2017-09-22T15:30:42Z20172017-01-01T00:00:00Zconference objectinfo:eu-repo/semantics/publishedVersionapplication/pdfhttp://hdl.handle.net/10198/14525engHalla, N.; Fernandes, Isabel P.; Heleno, S.A.; Calhelha, R.C.; Costa, P.; Rodrigues, A.E.; Boucherit, K.; Ferreira, I.C.F.R.; Barreiro, M.F. (2017). Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system. In XXV Encontro Nacional da Sociedade Portuguesa de Química. FFUL, Lisboa, Portugalinfo:eu-repo/semantics/openAccessreponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiainstacron:RCAAP2025-02-25T12:04:40Zoai:bibliotecadigital.ipb.pt:10198/14525Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireinfo@rcaap.ptopendoar:https://opendoar.ac.uk/repository/71602025-05-28T11:31:06.308771Repositórios Científicos de Acesso Aberto de Portugal (RCAAP) - FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiafalse
dc.title.none.fl_str_mv Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system
title Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system
spellingShingle Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system
Halla, Noureddine
Microencapsulation
Chitosan/TPP/vanillin
title_short Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system
title_full Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system
title_fullStr Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system
title_full_unstemmed Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system
title_sort Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system
author Halla, Noureddine
author_facet Halla, Noureddine
Fernandes, Isabel P.
Heleno, Sandrina A.
Calhelha, Ricardo C.
Costa, Patrícia
Rodrigues, Alírio
Boucherit, Kebir
Ferreira, Isabel C.F.R.
Barreiro, M.F.
author_role author
author2 Fernandes, Isabel P.
Heleno, Sandrina A.
Calhelha, Ricardo C.
Costa, Patrícia
Rodrigues, Alírio
Boucherit, Kebir
Ferreira, Isabel C.F.R.
Barreiro, M.F.
author2_role author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv Biblioteca Digital do IPB
dc.contributor.author.fl_str_mv Halla, Noureddine
Fernandes, Isabel P.
Heleno, Sandrina A.
Calhelha, Ricardo C.
Costa, Patrícia
Rodrigues, Alírio
Boucherit, Kebir
Ferreira, Isabel C.F.R.
Barreiro, M.F.
dc.subject.por.fl_str_mv Microencapsulation
Chitosan/TPP/vanillin
topic Microencapsulation
Chitosan/TPP/vanillin
description A. leucotrichus (Coss. & Dur.) Coss. & Dur., known in Algeria as “Kammûnes-sofi”, is a medicinal plant that finds culinary use by indigenous populations. Among others, it is used against stomach pain, indigestion, diarrhea, vomiting, fever, and to combat high blood pressure. In this work, the essential oil of A. leucotrichus, obtained by steam distillation (3h) from fruits collected in March 2015 from Tassili n'Ajjer, a vast plateau in south-east Algeria (25°30'0" N and 9°0'0" E), was chemically and biologically characterized and thereafter microencapsulated using a chitosan/TPP/vanillin system.
publishDate 2017
dc.date.none.fl_str_mv 2017-09-22T15:30:42Z
2017
2017-01-01T00:00:00Z
dc.type.driver.fl_str_mv conference object
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://hdl.handle.net/10198/14525
url http://hdl.handle.net/10198/14525
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv Halla, N.; Fernandes, Isabel P.; Heleno, S.A.; Calhelha, R.C.; Costa, P.; Rodrigues, A.E.; Boucherit, K.; Ferreira, I.C.F.R.; Barreiro, M.F. (2017). Microencapsulation of ammodaucus leucotrichus essential oil using chitosan/ TPP/vanillin chemical system. In XXV Encontro Nacional da Sociedade Portuguesa de Química. FFUL, Lisboa, Portugal
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.publisher.none.fl_str_mv SPQ
publisher.none.fl_str_mv SPQ
dc.source.none.fl_str_mv reponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron:RCAAP
instname_str FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron_str RCAAP
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reponame_str Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
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repository.mail.fl_str_mv info@rcaap.pt
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