Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis Processing

Bibliographic Details
Main Author: Lyubchyk, Sergiy
Publication Date: 2019
Other Authors: Shapovalova, Olesia, Lygina, Olena, Oliveira, Maria Conceiçao, Appazov, Nurbol, Lyubchyk, Andriy, Charmier, Adilia Januário, Lyubchik, Svetlana, Pombeiro, Armando J. L.
Format: Article
Language: eng
Source: Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
Download full: http://hdl.handle.net/10362/104936
Summary: Associate Laboratory for Green Chemistry (LAQV), which is financed by national funds from FCT/MCTES (UID/QUI/50006/2019).
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spelling Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis ProcessingGeneralSDG 7 - Affordable and Clean EnergyAssociate Laboratory for Green Chemistry (LAQV), which is financed by national funds from FCT/MCTES (UID/QUI/50006/2019).Many plants have medicinal properties due to substances known as phytochemicals. To utilize these plants in practice, numerous procedures, such as extraction, isolation and characterization methods and toxicology and bioactivity studies, must be designed and implemented. Integrated approach to process Carpobrotus edulis, a weed medicinal plant widely spread in Portugal, was developed into a closed loop of two processes: microwave assisted extraction (MAE) and activation (MAA), to produce both phytochemicals and biochar. The use of MAE for phytochemical extraction was shown to be more energy efficient than conventional Soxhlet extraction: the process time was decreased by 7–8 times, and the energy efficiency was increased by up to 97%. The yield of the extracts is of 27%. Qualitative and quantitative identification/characterization of the phytochemicals were performed by LC-MS and phytochemical screening assays. The results clearly indicated that Carpobrotus edulis is rich by flavonoids (up to 24%). The use of MAA to process the residual biomass could shorten the activation time, resulting in reduced energy consumption. Biochar with a high yield of 65% (on a biomass basis) and a well-developed texture (surface area of 68.9 m2/g; total pore volume of 0.10 cm3/g; micropore volume of 0.07 cm3/g) is obtained.LAQV@REQUIMTEUCIBIO - Applied Molecular Biosciences UnitUNINOVA-Instituto de Desenvolvimento de Novas TecnologiasCENIMAT-i3N - Centro de Investigação de Materiais (Lab. Associado I3N)DCM - Departamento de Ciência dos MateriaisRUNLyubchyk, SergiyShapovalova, OlesiaLygina, OlenaOliveira, Maria ConceiçaoAppazov, NurbolLyubchyk, AndriyCharmier, Adilia JanuárioLyubchik, SvetlanaPombeiro, Armando J. L.2020-09-29T22:22:54Z2019-12-012019-12-01T00:00:00Zinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articleapplication/pdfhttp://hdl.handle.net/10362/104936eng2045-2322PURE: 19005107https://doi.org/10.1038/s41598-019-53817-8info:eu-repo/semantics/openAccessreponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiainstacron:RCAAP2024-05-22T17:47:53Zoai:run.unl.pt:10362/104936Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireinfo@rcaap.ptopendoar:https://opendoar.ac.uk/repository/71602025-05-28T17:18:58.578514Repositórios Científicos de Acesso Aberto de Portugal (RCAAP) - FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiafalse
dc.title.none.fl_str_mv Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis Processing
title Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis Processing
spellingShingle Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis Processing
Lyubchyk, Sergiy
General
SDG 7 - Affordable and Clean Energy
title_short Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis Processing
title_full Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis Processing
title_fullStr Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis Processing
title_full_unstemmed Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis Processing
title_sort Integrated Green Chemical Approach to the Medicinal Plant Carpobrotus edulis Processing
author Lyubchyk, Sergiy
author_facet Lyubchyk, Sergiy
Shapovalova, Olesia
Lygina, Olena
Oliveira, Maria Conceiçao
Appazov, Nurbol
Lyubchyk, Andriy
Charmier, Adilia Januário
Lyubchik, Svetlana
Pombeiro, Armando J. L.
author_role author
author2 Shapovalova, Olesia
Lygina, Olena
Oliveira, Maria Conceiçao
Appazov, Nurbol
Lyubchyk, Andriy
Charmier, Adilia Januário
Lyubchik, Svetlana
Pombeiro, Armando J. L.
author2_role author
author
author
author
author
author
author
author
dc.contributor.none.fl_str_mv LAQV@REQUIMTE
UCIBIO - Applied Molecular Biosciences Unit
UNINOVA-Instituto de Desenvolvimento de Novas Tecnologias
CENIMAT-i3N - Centro de Investigação de Materiais (Lab. Associado I3N)
DCM - Departamento de Ciência dos Materiais
RUN
dc.contributor.author.fl_str_mv Lyubchyk, Sergiy
Shapovalova, Olesia
Lygina, Olena
Oliveira, Maria Conceiçao
Appazov, Nurbol
Lyubchyk, Andriy
Charmier, Adilia Januário
Lyubchik, Svetlana
Pombeiro, Armando J. L.
dc.subject.por.fl_str_mv General
SDG 7 - Affordable and Clean Energy
topic General
SDG 7 - Affordable and Clean Energy
description Associate Laboratory for Green Chemistry (LAQV), which is financed by national funds from FCT/MCTES (UID/QUI/50006/2019).
publishDate 2019
dc.date.none.fl_str_mv 2019-12-01
2019-12-01T00:00:00Z
2020-09-29T22:22:54Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://hdl.handle.net/10362/104936
url http://hdl.handle.net/10362/104936
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv 2045-2322
PURE: 19005107
https://doi.org/10.1038/s41598-019-53817-8
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv application/pdf
dc.source.none.fl_str_mv reponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron:RCAAP
instname_str FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron_str RCAAP
institution RCAAP
reponame_str Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
collection Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
repository.name.fl_str_mv Repositórios Científicos de Acesso Aberto de Portugal (RCAAP) - FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
repository.mail.fl_str_mv info@rcaap.pt
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