Modelagem matemática do processo de extração supercrítica de Humulus lupulus L. com CO2

Detalhes bibliográficos
Ano de defesa: 2015
Autor(a) principal: Kupski, Sergio Carlos lattes
Orientador(a): Palú, Fernando lattes
Banca de defesa: Palú, Fernando lattes, Borba, Carlos Eduardo lattes, Eyng, Eduardo lattes
Tipo de documento: Dissertação
Tipo de acesso: Acesso aberto
Idioma: por
Instituição de defesa: Universidade Estadual do Oeste do Paraná
Toledo
Programa de Pós-Graduação: Programa de Pós-Graduação em Engenharia Química
Departamento: Centro de Engenharias e Ciências Exatas
País: Brasil
Palavras-chave em Português:
CO2
Palavras-chave em Inglês:
Área do conhecimento CNPq:
Link de acesso: http://tede.unioeste.br/handle/tede/3995
Resumo: Supercritical fluid extraction (SFE) process of vegetable oils with CO2 is an alternative to the traditional processes, with advantages related to final product quality, extraction yield and simpler separation stages. Hops (Humulus Lupulus L.) are widely used for beer brewing and their essential oils contain substances with potential pharmaceutical use. Mathematical modeling of the mass transfer mechanisms that rule the SFE may provide information about the process parameters influence on the total yield and extraction rate. This work intends to analyze the influence of the following parameters: temperature (de 35 a 55º C), pressure (100 a 200 bar), particle size (de 3,28 X 10-4 m a 1,02 X 10-3 m), particle size distribution and raw material treatment. Extraction of hop with supercritical carbon dioxide was performed on experimental scale. The data obtained was used to adjust the extraction curves simulated with five models available at literature. Besides those, the data allowed to test a proposed model, applied for the extraction from hop bracts. Tested models adjusted the experimental data satisfactorily and the estimated parameters analysis allowed building another model.