Detalhes bibliográficos
| Ano de defesa: |
2010 |
| Autor(a) principal: |
OLIVEIRA, Alexandre Miranda de
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| Orientador(a): |
MAIA, Lauro June Queiroz
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| Banca de defesa: |
Não Informado pela instituição |
| Tipo de documento: |
Dissertação
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| Tipo de acesso: |
Acesso aberto |
| Idioma: |
por |
| Instituição de defesa: |
Universidade Federal de Goiás
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| Programa de Pós-Graduação: |
Mestrado em Física
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| Departamento: |
Ciências Exatas e da Terra
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| País: |
BR
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| Palavras-chave em Português: |
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| Palavras-chave em Inglês: |
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| Área do conhecimento CNPq: |
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| Link de acesso: |
http://repositorio.bc.ufg.br/tede/handle/tde/809
|
Resumo: |
This work is to study the crystallization of compounds in the form of post system alumina-yttria-silica prepared by sol-gel mixed methodology and Pechini. Powders (x / 2) Y ² ³ - (X / 2) Al ² O ³ - (1-x) SiO ² (x = 0.1 0.2, 0.3, 0.4 and 0.5 mol) were doped with erbium prepared and characterized. The physical properties of composite SiO ² ¹ YO-, 5 - AlO ¹, 5 were studied by x-ray diffraction, FTIR spectroscopy, thermogravimetry, differential thermal analysis and photoluminescence measurements. It was possible to maintain the amorphous compositions at high temperatures, no crystallization below 900 ° C and the formation of phase Y ² ² O7 Si at 1100 ° C. We obtained a reasonable life time of some compositions treated at 1000 ° C. We observed the emission of green upconversion to excite the samples with high power laser. All synthesized samples exhibit photoluminescence emission and have maximum emission at 1530 nm with a width of ~ 47nm. This broad issue is a desirable property for amplifiers used in systems division multiplexing wavelengths (WDM) and suggests that Er ³ + ions are hosted in the amorphous phase. |
