Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents
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| Yayın Tarihi: | 2024 |
| Diğer Yazarlar: | , , , , , |
| Materyal Türü: | Article |
| Dil: | eng |
| Kaynak: | Repositório Comum do Brasil - Deposita |
| Download full: | https://deposita.ibict.br/handle/deposita/690 |
Özet: | Hybrid naphthalenediimide/zinc phosphonate materials (NDI/Zn) were prepared by mixing solutions of N,N′-bis(2- phosphonoethyl)-1,4,5,8-naphthalenediimide (PNDI) and zinc nitrate, resulting in the precipitation of the desired compounds. Samples precipitated from water and N,N-dimethylformamide (DMF) were produced. The obtained samples had the expected elemental composition, and the presence of naphthalenediimides (NDI) was ascertained by infrared and UV−visible spectroscopy. All the samples were crystalline, according to powder X-ray diffraction. Nitrogen adsorption isotherms showed the presence of porosity in the NDI/Zn samples. Mesopores with a diameter = 4.1mm were present in the sample from DMF, with total pore volume reaching 0.13 cm3/g. |
| _version_ | 1870605173158576128 |
|---|---|
| author | Poly-Anna Vera Melo, Barbra |
| author2 | Fernando Gregório Junior, Denis Troilo de Oliveira, Matheus de Jesus Trindade, Fabiane van de Streek, Jacco Furlan Ferreira, Fabio Brochsztain, Sergio |
| author2_role | author author author author author author |
| author_browse | Brochsztain, Sergio Fernando Gregório Junior, Denis Furlan Ferreira, Fabio Poly-Anna Vera Melo, Barbra Troilo de Oliveira, Matheus de Jesus Trindade, Fabiane van de Streek, Jacco |
| author_facet | Poly-Anna Vera Melo, Barbra Fernando Gregório Junior, Denis Troilo de Oliveira, Matheus de Jesus Trindade, Fabiane van de Streek, Jacco Furlan Ferreira, Fabio Brochsztain, Sergio |
| author_role | author |
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| bitstream.url.fl_str_mv | https://deposita.ibict.br/bitstreams/879a9047-3323-4eba-b130-97b53fd6fbc7/download https://deposita.ibict.br/bitstreams/be3a62c6-314b-45ed-a014-47f26166128c/download https://deposita.ibict.br/bitstreams/067f4e3c-45fa-46a2-a8be-2ff068685dcf/download https://deposita.ibict.br/bitstreams/926e4020-d10e-431a-a564-9c55add0f7a3/download |
| collection | Repositório Comum do Brasil - Deposita |
| dc.contributor.author.fl_str_mv | Poly-Anna Vera Melo, Barbra Fernando Gregório Junior, Denis Troilo de Oliveira, Matheus de Jesus Trindade, Fabiane van de Streek, Jacco Furlan Ferreira, Fabio Brochsztain, Sergio |
| dc.date.accessioned.fl_str_mv | 2024-11-11T19:20:57Z |
| dc.date.issued.fl_str_mv | 2024 |
| dc.format.none.fl_str_mv | application/pdf application/pdf |
| dc.identifier.uri.fl_str_mv | https://deposita.ibict.br/handle/deposita/690 |
| dc.language.iso.fl_str_mv | eng |
| dc.publisher.country.fl_str_mv | Estados unidos |
| dc.publisher.none.fl_str_mv | Universidade Federal do ABC |
| dc.relation.ispartof.por.fl_str_mv | ACS Omega |
| dc.rights.driver.fl_str_mv | info:eu-repo/semantics/openAccess |
| dc.source.none.fl_str_mv | reponame:Repositório Comum do Brasil - Deposita instname:Instituto Brasileiro de Informação em Ciência e Tecnologia (Ibict) instacron:IBICT |
| dc.subject.cnpq.fl_str_mv | Química |
| dc.subject.eng.fl_str_mv | Metal Phosphonates Zinc Phosphonate Naphthalenediimides Mesoporous Materials |
| dc.title.por.fl_str_mv | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents |
| dc.type.driver.fl_str_mv | info:eu-repo/semantics/article |
| dc.type.status.fl_str_mv | info:eu-repo/semantics/publishedVersion |
| description | Hybrid naphthalenediimide/zinc phosphonate materials (NDI/Zn) were prepared by mixing solutions of N,N′-bis(2- phosphonoethyl)-1,4,5,8-naphthalenediimide (PNDI) and zinc nitrate, resulting in the precipitation of the desired compounds. Samples precipitated from water and N,N-dimethylformamide (DMF) were produced. The obtained samples had the expected elemental composition, and the presence of naphthalenediimides (NDI) was ascertained by infrared and UV−visible spectroscopy. All the samples were crystalline, according to powder X-ray diffraction. Nitrogen adsorption isotherms showed the presence of porosity in the NDI/Zn samples. Mesopores with a diameter = 4.1mm were present in the sample from DMF, with total pore volume reaching 0.13 cm3/g. |
| eu_rights_str_mv | openAccess |
| format | article |
| id | IBICT-1_16028042e78df1dc0c3a19e8ec65fa8e |
| instacron_str | IBICT |
| institution | IBICT |
| instname_str | Instituto Brasileiro de Informação em Ciência e Tecnologia (Ibict) |
| language | eng |
| network_acronym_str | IBICT-1 |
| network_name_str | Repositório Comum do Brasil - Deposita |
| oai_identifier_str | oai:deposita.ibict.br:deposita/690 |
| publishDate | 2024 |
| publishDateSort | 2024 |
| publisher.none.fl_str_mv | Universidade Federal do ABC |
| reponame_str | Repositório Comum do Brasil - Deposita |
| repository.mail.fl_str_mv | deposita@ibict.br |
| repository.name.fl_str_mv | Repositório Comum do Brasil - Deposita - Instituto Brasileiro de Informação em Ciência e Tecnologia (Ibict) |
| repository_id_str | 4658 |
| spelling | 2024-11-11T19:20:57Z2024https://deposita.ibict.br/handle/deposita/690Hybrid naphthalenediimide/zinc phosphonate materials (NDI/Zn) were prepared by mixing solutions of N,N′-bis(2- phosphonoethyl)-1,4,5,8-naphthalenediimide (PNDI) and zinc nitrate, resulting in the precipitation of the desired compounds. Samples precipitated from water and N,N-dimethylformamide (DMF) were produced. The obtained samples had the expected elemental composition, and the presence of naphthalenediimides (NDI) was ascertained by infrared and UV−visible spectroscopy. All the samples were crystalline, according to powder X-ray diffraction. Nitrogen adsorption isotherms showed the presence of porosity in the NDI/Zn samples. Mesopores with a diameter = 4.1mm were present in the sample from DMF, with total pore volume reaching 0.13 cm3/g.Hybrid naphthalenediimide/zinc phosphonate materials (NDI/Zn) were prepared by mixing solutions of N,N′-bis(2- phosphonoethyl)-1,4,5,8-naphthalenediimide (PNDI) and zinc nitrate, resulting in the precipitation of the desired compounds. Samples precipitated from water and N,N-dimethylformamide (DMF) were produced. The obtained samples had the expected elemental composition, and the presence of naphthalenediimides (NDI) was ascertained by infrared and UV−visible spectroscopy. All the samples were crystalline, according to powder X-ray diffraction. Nitrogen adsorption isotherms showed the presence of porosity in the NDI/Zn samples. Mesopores with a diameter = 4.1 nm were present in the sample from DMF, with total pore volume reaching 0.13 cm3/g.Fundação de Amparo à Pesquisa do Estado de São PauloSudeste-1application/pdfapplication/pdfengUniversidade Federal do ABCEstados unidosACS OmegaMetal PhosphonatesZinc PhosphonateNaphthalenediimidesMesoporous MaterialsQuímicaSynthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solventsinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article174817569Poly-Anna Vera Melo, BarbraFernando Gregório Junior, DenisTroilo de Oliveira, Matheusde Jesus Trindade, Fabianevan de Streek, JaccoFurlan Ferreira, FabioBrochsztain, Sergioinfo:eu-repo/semantics/openAccessreponame:Repositório Comum do Brasil - Depositainstname:Instituto Brasileiro de Informação em Ciência e Tecnologia (Ibict)instacron:IBICTTEXT(49) ACS Omega 2024.pdf.txtWritten by FormatFilter org.dspace.app.mediafilter.TikaTextExtractionFilter on 2025-06-06T20:15:37Z (GMT).Extracted texttext/plain49620https://deposita.ibict.br/bitstreams/879a9047-3323-4eba-b130-97b53fd6fbc7/downloadab72107991b26b543a83f5d07bc5af70MD53falseAnonymousREADTHUMBNAIL(49) ACS Omega 2024.pdf.jpgWritten by FormatFilter org.dspace.app.mediafilter.PDFBoxThumbnail on 2025-06-06T20:15:38Z (GMT).Generated Thumbnailimage/jpeg6616https://deposita.ibict.br/bitstreams/be3a62c6-314b-45ed-a014-47f26166128c/download69e609b59e0a89f38aa3debe1cb6543dMD54falseAnonymousREADLICENSElicense.txtWritten by org.dspace.content.LicenseUtilstext/plain; charset=utf-81867https://deposita.ibict.br/bitstreams/067f4e3c-45fa-46a2-a8be-2ff068685dcf/downloada7c148eec59885ba1ba6d14692be8465MD51falseAnonymousREADORIGINAL(49) ACS Omega 2024.pdf/dspace/deposita/upload/(49) ACS Omega 2024.pdfapplication/pdf7180988https://deposita.ibict.br/bitstreams/926e4020-d10e-431a-a564-9c55add0f7a3/downloadcbb9e6aef7ca1e4ff153c3034d800f06MD52trueAnonymousREADdeposita/6902026-03-20T17:39:59.353238Zopen.accessoai:deposita.ibict.br:deposita/690https://deposita.ibict.brRepositório ComumPUBhttp://deposita.ibict.br/oai/requestdeposita@ibict.bropendoar:46582026-03-20T17:39:59Repositório Comum do Brasil - Deposita - Instituto Brasileiro de Informação em Ciência e Tecnologia (Ibict)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 |
| spellingShingle | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents Poly-Anna Vera Melo, Barbra Metal Phosphonates Zinc Phosphonate Naphthalenediimides Mesoporous Materials Química |
| status_str | publishedVersion |
| title | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents |
| title_full | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents |
| title_fullStr | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents |
| title_full_unstemmed | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents |
| title_short | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents |
| title_sort | Synthesis and Characterization of Two Novel Naphthalenediimide/ Zinc Phosphonate Crystalline Materials Precipitated from Different Solvents |
| topic | Metal Phosphonates Zinc Phosphonate Naphthalenediimides Mesoporous Materials Química |
| url | https://deposita.ibict.br/handle/deposita/690 |