Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacic

Detalhes bibliográficos
Autor(a) principal: Amin,O.A.R.
Data de Publicação: 2011
Outros Autores: Belal,S.F., Bakry,R.
Tipo de documento: Artigo
Idioma: eng
Título da fonte: Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
Texto Completo: http://scielo.pt/scielo.php?script=sci_arttext&pid=S0872-19042011000200005
Resumo: Two sensitive voltammetric techniques (adsorptive and catalytic cathodic stripping) are described for the determination of timonacic, in the presence of copper or nickel ions, respectively. The measured peaks which correspond to the reduction or copper (I) or nickel - timonacic complexes are measured at -773 and -782 mV, respectively. The different experimental parameters have been carefully studied. The methods have been fully validated. The detection limits were 1.5 and 13.6 ng mL-1, respectively. The methods have been applied for the determination of timonacic in pharmaceutical tablets. The obtained results have been compared statistically with those obtained from a published method.
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spelling Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacictimonacicadsorptive stripping voltammetrycatalytic cathodic stripping voltammetrypharmaceutical tabletsTwo sensitive voltammetric techniques (adsorptive and catalytic cathodic stripping) are described for the determination of timonacic, in the presence of copper or nickel ions, respectively. The measured peaks which correspond to the reduction or copper (I) or nickel - timonacic complexes are measured at -773 and -782 mV, respectively. The different experimental parameters have been carefully studied. The methods have been fully validated. The detection limits were 1.5 and 13.6 ng mL-1, respectively. The methods have been applied for the determination of timonacic in pharmaceutical tablets. The obtained results have been compared statistically with those obtained from a published method.Sociedade Portuguesa de Electroquímica2011-01-01info:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/articletext/htmlhttp://scielo.pt/scielo.php?script=sci_arttext&pid=S0872-19042011000200005Portugaliae Electrochimica Acta v.29 n.2 2011reponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiainstacron:RCAAPenghttp://scielo.pt/scielo.php?script=sci_arttext&pid=S0872-19042011000200005Amin,O.A.R.Belal,S.F.Bakry,R.info:eu-repo/semantics/openAccess2024-02-06T17:07:07Zoai:scielo:S0872-19042011000200005Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireinfo@rcaap.ptopendoar:https://opendoar.ac.uk/repository/71602025-05-28T12:56:28.548042Repositórios Científicos de Acesso Aberto de Portugal (RCAAP) - FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiafalse
dc.title.none.fl_str_mv Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacic
title Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacic
spellingShingle Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacic
Amin,O.A.R.
timonacic
adsorptive stripping voltammetry
catalytic cathodic stripping voltammetry
pharmaceutical tablets
title_short Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacic
title_full Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacic
title_fullStr Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacic
title_full_unstemmed Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacic
title_sort Adsorptive and Catalytic Cathodic Stripping Voltammetric Determination of Timonacic
author Amin,O.A.R.
author_facet Amin,O.A.R.
Belal,S.F.
Bakry,R.
author_role author
author2 Belal,S.F.
Bakry,R.
author2_role author
author
dc.contributor.author.fl_str_mv Amin,O.A.R.
Belal,S.F.
Bakry,R.
dc.subject.por.fl_str_mv timonacic
adsorptive stripping voltammetry
catalytic cathodic stripping voltammetry
pharmaceutical tablets
topic timonacic
adsorptive stripping voltammetry
catalytic cathodic stripping voltammetry
pharmaceutical tablets
description Two sensitive voltammetric techniques (adsorptive and catalytic cathodic stripping) are described for the determination of timonacic, in the presence of copper or nickel ions, respectively. The measured peaks which correspond to the reduction or copper (I) or nickel - timonacic complexes are measured at -773 and -782 mV, respectively. The different experimental parameters have been carefully studied. The methods have been fully validated. The detection limits were 1.5 and 13.6 ng mL-1, respectively. The methods have been applied for the determination of timonacic in pharmaceutical tablets. The obtained results have been compared statistically with those obtained from a published method.
publishDate 2011
dc.date.none.fl_str_mv 2011-01-01
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://scielo.pt/scielo.php?script=sci_arttext&pid=S0872-19042011000200005
url http://scielo.pt/scielo.php?script=sci_arttext&pid=S0872-19042011000200005
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv http://scielo.pt/scielo.php?script=sci_arttext&pid=S0872-19042011000200005
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv text/html
dc.publisher.none.fl_str_mv Sociedade Portuguesa de Electroquímica
publisher.none.fl_str_mv Sociedade Portuguesa de Electroquímica
dc.source.none.fl_str_mv Portugaliae Electrochimica Acta v.29 n.2 2011
reponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron:RCAAP
instname_str FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron_str RCAAP
institution RCAAP
reponame_str Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
collection Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
repository.name.fl_str_mv Repositórios Científicos de Acesso Aberto de Portugal (RCAAP) - FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
repository.mail.fl_str_mv info@rcaap.pt
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