Image Recording and Processing Chemical Synthesis

Bibliographic Details
Main Author: Sousa, David M.
Publication Date: 2021
Other Authors: Carlos Lima, João, Ferreira, Isabel
Format: Article
Language: eng
Source: Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
Download full: http://hdl.handle.net/10362/169261
Summary: This work was mainly funded by ERC‐CoG‐2014, ChapTherPV, 647596 and partially by H2020‐ICT‐2014‐1, RIA, TransFlexTeg, 645241, FEDER funds through the COMPETE 2020 Program and National Funds through FCT – Portuguese Foundation for Science and Technology with the reference SFRH/BD/135948/2018. Publisher Copyright: © 2020 The Authors. Published by Wiley-VCH GmbH.
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spelling Image Recording and Processing Chemical SynthesisMethod Description and Demonstrationautomationfeature extractionimagingrecordingreproducibilitysynthesis parametersElectrochemistrySpectroscopyCatalysisFluid Flow and Transfer ProcessesThis work was mainly funded by ERC‐CoG‐2014, ChapTherPV, 647596 and partially by H2020‐ICT‐2014‐1, RIA, TransFlexTeg, 645241, FEDER funds through the COMPETE 2020 Program and National Funds through FCT – Portuguese Foundation for Science and Technology with the reference SFRH/BD/135948/2018. Publisher Copyright: © 2020 The Authors. Published by Wiley-VCH GmbH.The reproducibility of chemical synthesis is of crucial importance for both chemical industry and research. The development of simple yet robust methods and algorithms that generate a set of data to help the community access their method's reproducibility is desirable. We report a method for obtaining, processing and analyzing recorded images, using scripting language Python 3, from any camera that allows continuous visualization and recording of a chemical synthesis. The method can be used to assert synthesis reproducibility, to capture reaction events that might elude the naked eye and later be isolated in posterior reactions, to refine synthesis parameters such as temperature, microwave power and time and also to understand chemical reactions during synthesis. The method was exemplified with two microwave-assisted synthesis, zinc sulfide and silver sulfide, processed at our lab and applied to videos from other authors.CENIMAT-i3N - Centro de Investigação de Materiais (Lab. Associado I3N)DCM - Departamento de Ciência dos MateriaisDQ - Departamento de QuímicaLAQV@REQUIMTERUNSousa, David M.Carlos Lima, JoãoFerreira, Isabel2024-07-01T22:32:52Z2021-032021-03-01T00:00:00Zinfo:eu-repo/semantics/publishedVersioninfo:eu-repo/semantics/article5application/pdfhttp://hdl.handle.net/10362/169261engPURE: 94066643https://doi.org/10.1002/cmtd.202000043info:eu-repo/semantics/openAccessreponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiainstacron:RCAAP2025-04-21T01:32:40Zoai:run.unl.pt:10362/169261Portal AgregadorONGhttps://www.rcaap.pt/oai/openaireinfo@rcaap.ptopendoar:https://opendoar.ac.uk/repository/71602025-05-28T18:36:23.549952Repositórios Científicos de Acesso Aberto de Portugal (RCAAP) - FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologiafalse
dc.title.none.fl_str_mv Image Recording and Processing Chemical Synthesis
Method Description and Demonstration
title Image Recording and Processing Chemical Synthesis
spellingShingle Image Recording and Processing Chemical Synthesis
Sousa, David M.
automation
feature extraction
imaging
recording
reproducibility
synthesis parameters
Electrochemistry
Spectroscopy
Catalysis
Fluid Flow and Transfer Processes
title_short Image Recording and Processing Chemical Synthesis
title_full Image Recording and Processing Chemical Synthesis
title_fullStr Image Recording and Processing Chemical Synthesis
title_full_unstemmed Image Recording and Processing Chemical Synthesis
title_sort Image Recording and Processing Chemical Synthesis
author Sousa, David M.
author_facet Sousa, David M.
Carlos Lima, João
Ferreira, Isabel
author_role author
author2 Carlos Lima, João
Ferreira, Isabel
author2_role author
author
dc.contributor.none.fl_str_mv CENIMAT-i3N - Centro de Investigação de Materiais (Lab. Associado I3N)
DCM - Departamento de Ciência dos Materiais
DQ - Departamento de Química
LAQV@REQUIMTE
RUN
dc.contributor.author.fl_str_mv Sousa, David M.
Carlos Lima, João
Ferreira, Isabel
dc.subject.por.fl_str_mv automation
feature extraction
imaging
recording
reproducibility
synthesis parameters
Electrochemistry
Spectroscopy
Catalysis
Fluid Flow and Transfer Processes
topic automation
feature extraction
imaging
recording
reproducibility
synthesis parameters
Electrochemistry
Spectroscopy
Catalysis
Fluid Flow and Transfer Processes
description This work was mainly funded by ERC‐CoG‐2014, ChapTherPV, 647596 and partially by H2020‐ICT‐2014‐1, RIA, TransFlexTeg, 645241, FEDER funds through the COMPETE 2020 Program and National Funds through FCT – Portuguese Foundation for Science and Technology with the reference SFRH/BD/135948/2018. Publisher Copyright: © 2020 The Authors. Published by Wiley-VCH GmbH.
publishDate 2021
dc.date.none.fl_str_mv 2021-03
2021-03-01T00:00:00Z
2024-07-01T22:32:52Z
dc.type.status.fl_str_mv info:eu-repo/semantics/publishedVersion
dc.type.driver.fl_str_mv info:eu-repo/semantics/article
format article
status_str publishedVersion
dc.identifier.uri.fl_str_mv http://hdl.handle.net/10362/169261
url http://hdl.handle.net/10362/169261
dc.language.iso.fl_str_mv eng
language eng
dc.relation.none.fl_str_mv PURE: 94066643
https://doi.org/10.1002/cmtd.202000043
dc.rights.driver.fl_str_mv info:eu-repo/semantics/openAccess
eu_rights_str_mv openAccess
dc.format.none.fl_str_mv 5
application/pdf
dc.source.none.fl_str_mv reponame:Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
instname:FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron:RCAAP
instname_str FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
instacron_str RCAAP
institution RCAAP
reponame_str Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
collection Repositórios Científicos de Acesso Aberto de Portugal (RCAAP)
repository.name.fl_str_mv Repositórios Científicos de Acesso Aberto de Portugal (RCAAP) - FCCN, serviços digitais da FCT – Fundação para a Ciência e a Tecnologia
repository.mail.fl_str_mv info@rcaap.pt
_version_ 1833597539666886656

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